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Browsing by Subject "Electrophoresis, Capillary"

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    • Article  

      Analysis of polyphenols using capillary zone electrophoresis - Determination of the most effective wine sample pre-treatment method 

      Nicolaou, I. N.; Kapnissi‐Christodoulou, Constantina P. (2010)
      A simple CZE method has been developed for the simultaneous determination of eight polyphenolic compounds. The influence of several experimental conditions such as buffer (concentration and pH) and temperature were studied. ...

    • Article  

      Analytical separations in open-tubular capillary electrochromatography 

      Kapnissi‐Christodoulou, Constantina P.; Zhu, X.; Warner, I. M. (2003)
      This review represents a summary of recent progress in open-tubular capillary electro-chromatography (OT-CEC) for chiral and achiral separations. The OT-CEC approach is an alternative to packed-CEC that could eliminate the ...

    • Article  

      Analytical separations using molecular micelles in open-tubular capillary electrochromatography 

      Kapnissi‐Christodoulou, Constantina P.; Akbay, C.; Schlenoff, J. B.; Warner, I. M. (2002)
      Open-tubular capillary electrochromatography (OT-CEC) is an alternative approach to conventional CEC. The primary advantage of OT-CEC is the elimination of problems associated with frits and silica particles in conventional ...

    • Article  

      Chiral ionic liquids in chromatographic and electrophoretic separations 

      Kapnissi‐Christodoulou, Constantina P.; Stavrou, Ioannis J.; Mavroudi, Maria C. (2014)
      This report provides an overview of the application of chiral ionic liquids (CILs) in separation technology, and particularly in capillary electrophoresis and both gas and liquid chromatography. There is a large number of ...

    • Article  

      Chiral selectors in CE: Recent developments and applications 

      Tsioupi, Despina A.; Stefan-van Staden, R. -I; Kapnissi‐Christodoulou, Constantina P. (2013)
      This review article provides an overview of the recent advances in enantioanalysis by use of electrophoretic techniques. Due to the big number of publications in the subject mentioned above, this article is focused on ...

    • Article  

      Chiral selectors in CE: Recent developments and applications (2012-mid 2014) 

      Stavrou, Ioannis J.; Mavroudi, Maria C.; Kapnissi‐Christodoulou, Constantina P. (2015)
      There is a large number of chiral selectors (CSs) that have, over the years, been synthesized and used in electrophoretic enantioseparations. This report highlights the most important CSs applied in CE during the period ...

    • Article  

      Chiral separation of Huperzine A using CE - Method validation and application in pharmaceutical formulations 

      Tsioupi, Despina A.; Nicolaou, I. N.; Moore, L.; Kapnissi‐Christodoulou, Constantina P. (2012)
      The aim of this work is the development, validation and application of an MEKC method for the chiral separation of Huperzine A. Huperzine A is an important compound that is used to treat Alzheimer's disease. However, only ...

    • Article  

      Chiral separation of the clinically important compounds fucose and pipecolic acid using ce: Determination of the most effective chiral selector 

      Hadjistasi, Christoforos A.; Stavrou, Ioannis J.; Stefan-Van Staden, R. -I; Aboul‐Enein, Hassan Y.; Kapnissi‐Christodoulou, Constantina P. (2013)
      In this study, simple electrophoretic methods were developed for the chiral separation of the clinically important compounds fucose and pipecolic acid. In recent years, these analytes, and particularly their individual ...

    • Article  

      Combined use of cyclofructans and an amino acid ester-based ionic liquid for the enantioseparation of huperzine A and coumarin derivatives in CE 

      Stavrou, Ioannis J.; Breitbach, Z. S.; Kapnissi‐Christodoulou, Constantina P. (2015)
      Cyclofructans (CFs) and their derivatives have recently been proven to be efficient chiral selectors (CSs) for the enantioseparation of several analytes in CE, HPLC, and GC. In this study, the chiral separation ability of ...

    • Article  

      Combined use of l-alanine tert butyl ester lactate and trimethyl-ß-cyclodextrin for the enantiomeric separations of 2-arylpropionic acids nonsteroidal anti-inflammatory drugs 

      Mavroudi, Maria C.; Kapnissi‐Christodoulou, Constantina P. (2015)
      In this study, a new CE method, employing a binary system of trimethyl-ß-CD (TM-ß-CD) and a chiral amino acid ester-based ionic liquid (AAIL), was developed for the chiral separation of seven 2-arylpropionic acid nonsteroidal ...

    • Article  

      Development of a capillary electrophoresis-mass spectrometry method for the determination of rivastigmine in human plasma - Optimization of the limits of detection and quantitation 

      Nicolaou, I. N.; Kapnissi‐Christodoulou, Constantina P. (2012)
      A capillary zone electrophoresis-electrospray ionization-mass spectrometry (CZE-ESI-MS) method was developed for the analysis of the acetylcholinesterase inhibitor rivastigmine. Several electrophoretic and ESI-MS parameters ...

    • Article  

      Evaluation of amino acid ester-based ionic liquids as buffer additives in CE for the separation of 2-arylpropionic acids nonsteroidal anti-inflammatory drugs 

      Mavroudi, Maria C.; Kapnissi‐Christodoulou, Constantina P. (2014)
      The aim of the present study is the CE performance evaluation for the separation of 2-arylpropionic acid nonsteroidal anti-inflammatory drugs. In particular, the separation of indoprofen, carprofen, ketoprofen, ibuprofen, ...

    • Article  

      Open-tubular capillary electrochromatography using a polymeric surfactant coating 

      Kamande, M. W.; Kapnissi‐Christodoulou, Constantina P.; Zhu, X.; Akbay, C.; Warner, I. M. (2003)
      A stable polyelectrolyte multilayer (PEM) coating was investigated for use in open-tubular capillary electrochromatography (o-CEC). In this approach, the PEM consisted of the cationic polymer of a quaternary ammonium salt, ...

    • Article  

      Open-tubular capillary electrochromatography/electrospray ionization-mass spectrometry using polymeric surfactant as a stationary phase coating 

      Zhu, X.; Kamande, M. W.; Thiam, S.; Kapnissi‐Christodoulou, Constantina P.; Mwongela, S. M.; Warner, I. M. (2004)
      We describe the use of the polymeric surfactant poly(sodium undecylenic sulfate) (poly-SUS) as a stationary phase coating in open-tubular capillary electrochromatog raphy (OT-CEC) coupled with electrospray ionization-mass ...

    • Article  

      Use of chiral amino acid ester-based ionic liquids as chiral selectors in CE 

      Stavrou, Ioannis J.; Kapnissi‐Christodoulou, Constantina P. (2013)
      In this study, the applicability of a chiral ionic liquid (CIL) as the sole chiral selector in CE was investigated for the first time. In particular, five amino acid ester-based CILs were synthesized and used as additives ...

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