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Browsing by Subject "Nuclear magnetic resonance spectroscopy"

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Now showing items 1-20 of 33

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    • Article  

      ABC triblock polymethacrylates: Group transfer polymerization synthesis of the ABC, ACB, and BAC topological isomers and solution characterization 

      Patrickios, Costas S.; Lowe, A. B.; Armes, S. P.; Billingham, N. C. (1998)
      ABC triblock copolymers of methyl methacrylate (MMA), (dimethylamino)-ethyl methacrylate (DMAEMA), and tetrahydropyranyl methacrylate (THPMA) consisting of 12 units of each type of monomer were synthesized by group transfer ...

    • Article  

      ABC Triblock Terpolymers with Orthogonally Deprotectable Blocks: Synthesis, Characterization, and Deprotection 

      Elladiou, Marios; Patrickios, Costas S. (2015)
      The development and availability of new protecting groups are vital for all branches of synthetic chemistry. Equally vital is the facile and selective removal of these groups, leaving intact other protecting groups which ...

    • Article  

      Alternating amphiphilic multiblock copolymers: Controlled synthesis via RAFT polymerization and aqueous solution characterization 

      Hadjiantoniou, N. A.; Krasia-Christoforou, T.; Loizou, E.; Porcar, L.; Patrickios, C. S. (2010)
      Four linear amphiphilic multiblock copolymers based on 2-(dimethylamino) ethyl methacrylate (DMAEMA, hydrophilic) and methyl methacrylate (MMA, hydrophobic), bearing from two to five blocks, were synthesized using reversible ...

    • Article  

      Alternating amphiphilic multiblock copolymers: Controlled synthesis via RAFT polymerization and aqueous solution characterization 

      Hadjiantoniou, Natalie A.; Krasia‐Christoforou, Theodora; Loizou, Elena; Porcar, L.; Patrickios, Costas S. (2010)
      Four linear amphiphilic multiblock copolymers based on 2-(dimethylamino) ethyl methacrylate (DMAEMA, hydrophilic) and methyl methacrylate (MMA, hydrophobic), bearing from two to five blocks, were synthesized using reversible ...

    • Article  

      Amphiphilic model conetworks based on combinations of methacrylate, acrylate, and styrenic units: Synthesis by RAFT radical polymerization and characterization of the swelling behavior 

      Achilleos, Mariliz; Krasia‐Christoforou, Theodora; Patrickios, Costas S. (2007)
      Reversible addition-fragmentation chain transfer (RAFT) polymerization was employed for the preparation of homopolymer and copolymer (co)networks based on four monomer units, belonging to three monomer types: methacrylates, ...

    • Article  

      Amphiphilic model conetworks based on combinations of methacrylate, acrylate, and styrenic units: Synthesis by RAFT radical polymerization and characterization of the swelling behavior 

      Achilleos, M.; Krasia-Christoforou, T.; Patrickios, C. S. (2007)
      Reversible addition-fragmentation chain transfer (RAFT) polymerization was employed for the preparation of homopolymer and copolymer (co)networks based on four monomer units, belonging to three monomer types: methacrylates, ...

    • Article  

      Amphiphilic model conetworks based on cross-linked star copolymers of benzyl methacrylate and 2-(dimenthylamino)ethyl methacrylate: Synthesis, characterization, and DNA adsorption studies 

      Achilleos, Demetra S.; Georgiou, Theoni K.; Patrickios, Costas S. (2006)
      Six amphiphilic model conetworks of a new structure, that of cross-linked "in-out" star copolymers, were synthesized by the group transfer polymerization (GTP) of the hydrophobic monomer benzyl methacrylate (BzMA) and the ...

    • Article  

      Amphiphilic polymethacrylate model co-networks: Synthesis by RAFT radical polymerization and characterization of the swelling behavior 

      Krasia-Christoforou, T.; Patrickios, C. S. (2006)
      Reversible addition-fragmentation chain transfer (RAFT) controlled radical polymerization was employed, for the first time, to prepare well-defined (model) amphiphilic polymer co-networks based on n-butyl methacrylate ...

    • Article  

      Amphiphilic polymethacrylate model co-networks: Synthesis by RAFT radical polymerization and characterization of the swelling behavior 

      Krasia‐Christoforou, Theodora; Patrickios, Costas S. (2006)
      Reversible addition-fragmentation chain transfer (RAFT) controlled radical polymerization was employed, for the first time, to prepare well-defined (model) amphiphilic polymer co-networks based on n-butyl methacrylate ...

    • Article  

      End-linked semifluorinated amphiphilic polymer conetworks: Synthesis by sequential reversible addition - Fragmentation chain transfer polymerization and characterization 

      Pafiti, Kyriaki S.; Loizou, Elena; Patrickios, Costas S.; Porcar, L. (2010)
      One-pot, sequential reversible addition - fragmentation chain transfer (RAFT) polymerization was employed for the preparation of five end-linked semifluorinated amphiphilic polymer conetworks based on 2,2,2-trifluoroethyl ...

    • Article  

      From colloidal aggregates to layered nanosized structures in polymer-surfactant systems. 1. Basic phenomena 

      Leontidis, Epameinondas; Kyprianidou-Leodidou, Tasoula; Caseri, Walter; Robyr, P.; Krumeich, F.; Kyriacou, Kyriacos C. (2001)
      In this work, we examine the rich crystallization behavior that occurs in PbII/S-II/poly(ethylene oxide) (PEO)/sodium dodecyl sulfate (SDS) systems, in which the anionic surfactant interacts strongly with the polymer ...

    • Article  

      High-molecular-weight symmetrical multiblock copolymers: Synthesis by RAFT polymerization and characterization 

      Pafiti, Kyriaki S.; Patrickios, Costas S.; Abetz, Clarissa; Abetz, Volker (2013)
      High-molecular-weight (MW) symmetrical multiblock copolymers, based on the hydrophobic monomers styrene (Sty) and methyl methacrylate (MMA), and the more polar monomer, 2-vinyl pyridine (2VPy), were prepared using stepwise ...

    • Article  

      Liquid-crystalline phase behavior in a zwitterionic tetraazapentacene 

      Riley, A. E.; Mitchell, G. W.; Koutentis, Panayiotis Andreas; Bendikov, M.; Kaszynki, P.; Wudl, F.; Tolbert, S. H. (2003)
      A 5,7-dioctadecylquinoxalinophenazine zwitterion 1 has been investigated to determine its thermal phase behavior. A combination of differential scanning calorimetry (DSC), variable temperature low- and high-angle X-ray ...

    • Article  

      Near-monodisperse, n-alkyl, end-functionalized poly(methyl vinyl ether)s: Synthesis by living cationic polymerization and solution characterization 

      Patrickios, Costas S.; Forder, C.; Armes, S. P.; Billingham, N. C. (1998)
      Water-soluble amphiphilic diblock copolymers were synthesized by the living cationic polymerization of methyl vinyl ether (hydrophilic block) and its subsequent termination with n-alcohols of chain lengths varying from one ...

    • Article  

      New antimony(III) halide complexes with dithiocarbamate ligands derived from thiuram degradation: The effect of the molecule's close contacts on in vitro cytotoxic activity 

      Urgut, O. S.; Ozturk, I. I.; Banti, Christina N.; Kourkoumelis, Nikolaos; Manoli, Maria; Tasiopoulos, Anastasios J.; Hadjikakou, Sotiris K. (2016)
      Antimony(III) halide complexes of the formulae {[SbBr(Me2DTC)2]n} (1), {[SbI(Me2DTC)2]n} (2) and {[(Me2DTC)2Sb(μ2-I)Sb(Me2DTC)2]+.I3-} (3) (Me2DTC = dimethyldithiocarbomate) were synthesized from SbX3, (X = Br or I) and ...

    • Article  

      Reaction of tetracyanoethylene with SCl1 

      Koutentis, Panayiotis Andreas; Rces, C. W. (2000)
      The chloride ion catalysed addition of SCl2 to TCNE gives the 4-dicyanomethylene-l,2,6-thiadiazine 2 (60%) with two minor products (5%) of extensive molecular rearrangement, the pyrimidine 4 and the pyrroloimidazothiadiazine ...

    • Article  

      Synthesis and aqueous solution characterization of amphiphilic diblock copolymers containing carbazole 

      Krasia-Christoforou, T.; Patrickios, C. S. (2002)
      A series of near-monodisperse diblock copolymers of 2-(N-carbazolyl)ethyl methacrylate and 2-(dimethylamino)ethyl methacrylate (DMAEMA) of relatively low molecular weights (2600-24,000 g mol-1) were synthesized by group ...

    • Article  

      Synthesis and aqueous solution characterization of amphiphilic diblock copolymers containing carbazole 

      Krasia‐Christoforou, Theodora; Patrickios, Costas S. (2002)
      A series of near-monodisperse diblock copolymers of 2-(N-carbazolyl)ethyl methacrylate and 2-(dimethylamino)ethyl methacrylate (DMAEMA) of relatively low molecular weights (2600-24,000 g mol-1) were synthesized by group ...

    • Article  

      Synthesis and aqueous solution characterization of catalytically active block copolymers containing imidazole 

      Simmons, M. R.; Patrickios, Costas S. (1998)

    • Article  

      Synthesis and aqueous solution characterization of dihydrophilic block copolymers of methyl vinyl ether and methyl triethylene glycol vinyl ether 

      Forder, C.; Patrickios, Costas S.; Armes, S. P.; Billingham, N. C. (1996)
      Water-soluble dihydrophilic AB block copolymers of methyl vinyl ether (MVE) and methyl triethylene glycol vinyl ether (MTEGVE) were synthesized by living cationic polymerization, with copolymer molecular weights in the ...

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