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Browsing by Subject "Organometallic Compounds"

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    • Article  

      Employment of methyl 2-pyridyl ketone oxime in manganese non-carboxylate chemistry: MnII2MnIV and MnII 2MnIII6 complexes 

      Stoumpos, Constantinos C.; Stamatatos, Theocharis C.; Sartzi, H.; Roubeau, O.; Tasiopoulos, Anastasios J.; Nastopoulos, Vassilios; Teat, S. J.; Christou, George; Perlepes, Spyros P. (2009)
      The employment of the anion of methyl 2-pyridyl ketone oxime (mpko -) as a tridentate chelating/bridging ligand in manganese chemistry is described. The inorganic anion (Br-, ClO4-) used in the reaction affects the identity ...

    • Article  

      High nuclearity single-molecule magnets: A mixed-valence Mn26 cluster containing the di-2-pyridylketone diolate dianion 

      Stamatatos, Theocharis C.; Nastopoulos, Vassilios; Tasiopoulos, Anastasios J.; Moushi, Eleni E.; Wernsdorfer, W.; Christou, George; Perlepes, Spyros P. (2008)
      The employment of the dianion (dpkd2-) of the gem-diol form of di-2-pyridylketone (dpk) as a tetradentate chelate in manganese chemistry is reported, and the synthesis, crystal structure, and magnetochemical characterization ...

    • Article  

      Identification of a potent activator of Akt phosphorylation from a novel series of phenolic, picolinic, pyridino, and hydroxamic zinc(II) complexes 

      Georgiades, Savvas N.; Mak, L. H.; Angurell, I.; Rosivatz, E.; Firouz Mohd Mustapa, M.; Polychroni, Christoulla; Woscholski, R.; Vilar, R. (2011)
      The discovery of small-molecule modulators of signaling pathways is currently a particularly active area of research. We aimed at developing unprecedented metal-based activators of Akt signaling which can potentially find ...

    • Article  

      Is vanadate reduced by thiols under biological conditions? Changing the Redox potential of V(V)/V(IV) by complexation in aqueous solution 

      Crans, D. C.; Zhang, B.; Gaidamauskas, E.; Keramidas, Anastasios D.; Willsky, G. R.; Roberts, C. R. (2010)
      Although dogma states that vanadate is readily reduced by glutathione, cysteine, and other thiols, there are several examples documenting that vanadium(V)-sulfur complexes can form and be observed. This conundrum has ...

    • Article  

      Monomeric compounds containing the cis-[V(=O)(OH)]+ core 

      Tolis, Evangelos I.; Manos, Manolis J.; Tasiopoulos, Anastasios J.; Raptopoulou, Catherine P.; Terzis, Aris; Sigalas, Michael P.; Deligiannakis, Yiannis G.; Kabanos, Themistoklis A. (2002)
      HYSCORE with a vanadium core: Examples of monomeric metal compounds containing the cis-[M(=O)(OH)]n+ unit, namely the VIVO2+ complexes [VIVO(OH)(bipy)2]BF4 (1

    • Article  

      New antimony(III) bromide complexes with thioamides: Synthesis, characterization, and cytostatic properties 

      Ozturk, I. I.; Hadjikakou, Sotiris K.; Hadjiliadis, Nick; Kourkoumelis, Nikolaos; Kubicki, Maciej; Tasiopoulos, Anastasios J.; Scleiman, H.; Barsan, M. M.; Butler, I. S.; Balzarini, J. (2009)
      New antimony(III) bromide complexes with the heterocyclic thioamides, thiourea (TU), 2-mercapto-1-methylimidazole (MMl), 2-mercapto-benzimidazole (MBZlM), 2-mercapto-5-methyl-benzimidazole (MMBZIM), 5-ethoxy-2-mercapto- ...

    • Article  

      Novel lipophilic amidate oxorhenium and oxotechnetium complexes as potential brain agents: Synthesis, characterization and biological evaluation 

      Papadopoulos, Minas S.; Nock, B.; Maina-Nock, Theodosia; Pirmettis, Ioannis C.; Raptopoulou, Catherine P.; Tasiopoulos, Anastasios J.; Troganis, Anastassios N.; Kabanos, Themistoklis A.; Terzis, Aris; Chiotellis, Efstratios (2001)
      Novel oxorhenium and oxotechnetium complexes based on the tetradentate 1-(2-hydroxybenzamido)-2-(pyridinecarboxamido)benzene, H3L, ligand have been synthesized and characterized herein. Thus, by reacting equimolar quantities ...

    • Article  

      Solid state and aqueous solution characterization of rectangular tetranuclear VIV/V-p-semiquinonate/hydroquinonate complexes exhibiting a proton induced electron transfer 

      Drouza, Chryssoula; Keramidas, Anastasios D. (2008)
      Reaction of the non-innocent dinucleating ligand 2,5-bis[N,N- bis(carboxymethyl) arninomethyl]hydroquinone (H6bicah) with VO 2+ and VO43- salts in water in the pH range 2 to 4.5 provides a series of novel tetranuclear VIV ...

    • Article  

      Synthesis and structural characterization of new cu(I) complexes with the antithyroid drug 6-n-propyl-thiouracil. Study of the cu(I)-catalyzed intermolecular cycloaddition of iodonium ylides toward benzo[b]furans with pharmaceutical implementations 

      Paizanos, K.; Charalampou, D. C.; Kourkoumelis, Nikolaos; Kalpogiannaki, Dimitra; Hadjiarapoglou, Lazaros P.; Spanopoulou, A.; Lazarou, Konstantinos; Manos, Manolis J.; Tasiopoulos, Anastasios J.; Kubicki, Maciej; Hadjikakou, Sotiris K. (2012)
      The reaction of copper(I) iodide with 6-n-propylthiouracil (ptu) in the presence or absence of the triphenylphosphine (tpp) or tri(p-tolyl)phosphine (tptp) in a 1:1:2 molar ratio forms the mixed ligand Cu(I) complex with ...

    • Article  

      Synthesis of triazafluoranthenones via silver(I)-mediated nonoxidative and oxidative intramolecular palladium-catalyzed cyclizations 

      Koutentis, Panayiotis Andreas; Loizou, G.; Lo Re, D. (2011)
      Silver(I) fluoride (AgF)-mediated intramolecular nonoxidative and oxidative palladium-catalyzed cyclizations of 1,3-diphenyl- and 8-iodo-1,3- diphenylbenzo[e][1,2,4]triazin-7(1H)-ones 6a (R = H) and 7a (R = I) afford a new ...

    • Article  

      Synthesis, structure, magnetic properties and aqueous solution characterization of p-hydroquinone and phenol iminodiacetate copper(ii) complexes 

      Stylianou, M.; Drouza, C.; Viskadourakis, Z.; Giapintzakis, John; Keramidas, A. D. (2008)
      The reaction of Cu2+ acetate monohydrate with 2-[N,N′-bis(carboxymethyl)aminomethyl]-4-carboxyphenol (H 4cacp), 2-[N,N-bis(carboxymethyl)aminomethyl]hydroquinone (H 4cah) and the dinucleating 2,5-bis[N,N-bis(carboxymethy ...

    • Article  

      Synthesis, structure, magnetic properties and aqueous solution characterization of p-hydroquinone and phenol iminodiacetate copper(ii) complexes 

      Stylianou, Marios; Drouza, Chryssoula; Viskadourakis, Zacharias A.; Giapintzakis, Ioannis; Keramidas, Anastasios D. (2008)
      The reaction of Cu2+ acetate monohydrate with 2-[N,N′-bis(carboxymethyl)aminomethyl]-4-carboxyphenol (H 4cacp), 2-[N,N-bis(carboxymethyl)aminomethyl]hydroquinone (H 4cah) and the dinucleating 2,5-bis[N,N-bis(carboxymethy ...

    • Article  

      Two-step total syntheses of Canthin-6-one alkaloids: New one-pot sequential Pd-catalyzed Suzuki-Miyaura coupling and Cu-catalyzed amidation reaction 

      Gollner, A.; Koutentis, Panayiotis Andreas (2010)
      "Chemical Equation Presented" Canthin-6-one (1) and nine analogues including the naturally occurring 9-methoxycanthin-6-one (2) and amaroridine (3) are prepared rapidly and in high yields via a convergent "non-classical" ...

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