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Browsing by Subject "stereochemistry"

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    • Article  

      Glucose-based spiro-isoxazolines: A new family of potent glycogen phosphorylase inhibitors 

      Benltifa, Mahmoud; Hayes, Joseph M.; Vidal, Sébastien; Gueyrard, David; Goekjian, Peter G.; Praly, Jean Pierre; Kizilis, Gregory; Tiraidis, Costas; Alexacou, Kyra Melinda; Chrysina, Evangelia D.; Zographos, Spyros E.; Leonidas, Demetres D.; Archontis, Georgios Z.; Oikonomakos, Nikos G. (2009)
      A series of glucopyranosylidene-spiro-isoxazolines was prepared through regio- and stereoselective [3+2]-cycloaddition between the methylene acetylated exo-glucal and aromatic nitrile oxides. The deprotected cycloadducts ...

    • Article  

      A new [2 + 2] functionalization of C60 with alkyl-substituted 1,3- butadienes: A mechanistic approach. Stereochemistry and isotope effects 

      Vassilikogiannakis, G.; Chronakis, Nikos; Orfanopoulos, Michael (1998)
      The stereochemistry and secondary isotope effects of the [2 + 2] photocycloaddition of trans,trans- (7), cis,cis- (8), and cis,trans-2,4- hexadiene (9), 2,5-dimethyl-2,4-hexadiene (1), and its deuterated analogues 1-d1, ...

    • Article  

      Of ortho-conjugatively linked reactive intermediates: The cases of ortho-phenylene-(bis)nitrene, -carbenonitrene, and -(bis)carbene 

      Nicolaïdes, Andrew N.; Nakayama, T.; Yamazaki, K.; Tomioka, H.; Koseki, S.; Stracener, L. L.; McMahon, R. J. (1999)
      ortho-Phenylene-bisnitrene (2) and -carbenonitrene (3) were generated in an inert matrix at low temperature, characterized by IR spectroscopy, and identified with the help of DFT calculations. Their thermal and photochemical ...

    • Article  

      Regio- and stereoselective synthesis of enantiomerically pure [60]fullerene tris-adducts with an inherently chiral e,e,e addition pattern 

      Chronakis, Nikos; Hirsch, A. (2005)
      The synthesis and flash column chromatographic separation of c enantiomerically pure tris-adducts of C60 with an e,e,e-addition pattern is achieved via cyclopropanation with chiral D3-symmetrical cyclo-tris(malonate) ...

    • Article  

      Regioselective synthesis and zone selective deprotection of [60]fullerene tris-adducts with an e,e,e addition pattern 

      Beuerle, F.; Chronakis, Nikos; Hirsch, A. (2005)
      D3h-symmetrical tripodal tris(malonate) tethers have been used for the synthesis of [60]fullerene tris-adducts with an e,e,e addition pattern bearing topologically distinct polar and equatorial addend zones that can ...

    • Article  

      Remote functionalization of C60 with enantiomerically pure cyclo-[2]-malonate tethers bearing C12 and C14 spacers: Synthetic access to bisadducts of C60 with the inherently chiral trans-3 addition pattern 

      Riala, Maria; Chronakis, Nikos (2013)
      In this Article, we describe the synthesis of two optically pure diols bearing a 1,2-diol moiety masked as an isopropylidene acetal group and long alkyl chains comprised of 12 and 14 carbon atoms, respectively. The synthetic ...

    • Article  

      Ring opening of the cyclopropylcarbinyl radical and its N- and O- substituted analogues: A theoretical examination of very fast unimolecular reactions 

      Smith, D. M.; Nicolaïdes, Andrew N.; Golding, B. T.; Radom, L. (1998)
      High level ab initio molecular orbital calculations have been used to examine the ring opening of the cyclopropylcarbinyl radical and its heterosubstituted analogues. The applicability of various theoretical techniques to ...

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