Browsing by Subject "Scanning electron microscopy"
Now showing items 21-40 of 45
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Conference Object
Microstructure, mechanical and tribological properties of reactive magnetron sputtered titanium carbide coatings
(Affiliation: Dept. of Mechanical and Manufacturing Engineering, University of Cyprus, 1678, Nicosia, CyprusAffiliation: Dept. PA-ATM01/SGP21, Engineering Process Technology, Robert Bosch GmbH, Postfach 300220, 70442 Stuttgart, GermanyAffiliation: Dept. of Mechanical Science and Engineering, University of Illinois at Urbana-Champaign, Urbana, IL 61801, United StatesCorrespondence Address: Polycarpou, A. A.Dept. PA-ATM01/SGP21, Engineering Process Technology, Robert Bosch GmbH, Postfach 300220, 70442 Stuttgart, Germanyemail: polycarp@uiuc.edu, 2008)This study describes the correlation between the microstructure, mechanical and tribological properties of Ti 1-xCx coatings (with x being in the range of 0-0.5), deposited by reactive magnetron sputtering from a Ti target ...
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Article
MRI-based morphological modeling, synthesis and characterization of cardiac tissue-mimicking materials
(2012)This study uses standard synthetic methodologies to produce tissue-mimicking materials that match the morphology and emulate the in vivo murine and human cardiac mechanical and imaging characteristics, with dynamic mechanical ...
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Article
N2O decomposition over ceria-promoted Ir/Al2O3 catalysts: The role of ceria
(2016)The impact of CeO2 in the Al2O3-20wt% CeO2 support prepared by the co-precipitation method on the Ir particle size, morphology and oxidation state, and in turn on the deN2O catalytic activity (1000ppmN2O) of supported Ir ...
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Article
The nanostructure, wear and corrosion performance of arc-evaporated CrBxNy nanocomposite coatings
(2009)The composition, nanostructure, tribological and corrosion behaviour of reactive arc evaporated CrBxNy coatings have been studied and compared to CrN. The CrBxNy coatings were deposited on a commercial Oerlikon Balzers RCS ...
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Article
Preparation and characterization of a cerium(IV)-incorporated manganese oxide OMS-2. Effect of cerium(IV) template on octahedral molecular sieves of manganese oxide and characterization of manganese oxide molecular sieves with cerium(IV) as dopant
(2008)The manganese oxide material K-OMS-2 was synthesized both via a redox reaction between potassium permanganate and manganese nitrate in an acidic medium (nitric acid) under reflux conditions and by the sol-gel reaction ...
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Article
Pulsed-laser deposition of NiMnSb thin films at moderate temperatures
(2002)Thin films of the half-Heusler alloy NiMnSb, which is predicted by band-structure calculations to be a half-metallic ferromagnet, were grown on various substrates (Si and InAs) using pulsed-laser deposition. The growth ...
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Article
Raman spectroscopy using a fiber optic probe with subwavelength aperture
(1994)Raman spectroscopy with subwavelength spatial resolution of a diamond sample was recorded using a tapered fiber optical probe in conjunction with a conventional Raman spectrometer. The experiment demonstrates the potential ...
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Article
Rates of activation and scanning electron microscopy of polyarylamide-derived chars
(1995)Fibrous activated carbons were prepared from Kevlar® (poly (p-phenylene terephthalamide)) and Nomex® (poly (m-phenylene isophthalamide)) by carbonisation in nitrogen and subsequent activation in steam of carbon dioxide to ...
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Article
Regeneration of three-way automobile catalysts using biodegradable metal chelating agent-S, S-ethylenediamine disuccinic acid (S, S-EDDS)
(2011)Regeneration of the activity of three-way catalytic converters (TWCs) was tested for the first time using a biodegradable metal chelating agent (S, S-ethylenediamine disuccinic acid (S, S-EDDS). The efficiency of this novel ...
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Article
Room temperature synthesis and high temperature frictional study of silver vanadate nanorods
(2010)We report the room temperature (RT) synthesis of silver vanadate nanorods (consisting of mainly β-AgVO3) by a simple wet chemical route and their frictional study at high temperatures (HT). The sudden mixing of ammonium ...
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Article
Solid-state synthesis of Mg 2Si via short-duration ball-milling and low-temperature annealing
(2013)In this work, a short duration ball-milling of elemental Mg and Si followed by a thermal treatment is suggested in order to synthesize magnesium silicide via solid-state reaction. The formation of magnesium silicide was ...
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Solvothermal synthesis, nanostructural characterization and gas cryo-adsorption studies in a metal–organic framework (IRMOF-1) material
(2017)A nanoporous metal–organic framework material, exhibiting an IRMOF-1 type crystalline structure, was prepared by following a direct solvothermal synthesis approach, using zinc nitrate and terephthalic acid as precursors ...
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Conference Object
Stoichiometry issues in pulsed laser deposition of the ferromagnetic alloy NiMnSb
(Affiliation: NIRDO, BucharestAffiliation: MADIREL, Univ. Provence Centre St. Charles, Marseille, FranceAffiliation: Natl. Inst. Res. Devmt. Mat. Phy., BucharestAffiliation: Foundation for Res. and Technology, HELLAS, Inst. Electron. Structure and Laser, Heraklion, Crete, GreeceCorrespondence Address: Grigorescu, C.E.A.NIRDO, Bucharest, 2002)We report on the reproducible growth of stoichiometric thin films of ferromagnetic intermetallic compound NiMnSb by pulsed laser deposition (PLD) on various substrates. The films are grown at moderate temperature (around ...
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Article
Structural Characterization and Thermoelectric Properties of Hot-Pressed CoSi Nanocomposites
(2014)Fabrication of nanocomposites by introduction of SiO2 metal oxide nanoparticles into a cobalt silicide thermoelectric matrix is studied. The CoSi matrix material was prepared through solid-state synthesis, and the nano-SiO2 ...
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Article
Structural effects of crosslinking a biopolymer hydrogel derived from marine mussel adhesive protein
(2006)In an effort to explore new biocompatible substrates for biomedical technologies, we present a structural study on a crosslinked gelatinous protein extracted from marine mussels. Prior studies have shown the importance of ...
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Article
Structural features of ball-milled nanostructured K2Bi 8Se13 thermoelectric material
(2011)In this work, K2Bi8Se13 material was ball-milled in order to develop nanostructures through the modification of structural features. Structural changes during ball-milling were followed by powder X-ray diffraction measurements, ...
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Article
Structural, magnetic, and electrical properties of NiMnSb thin films grown on InSb by pulsed-laser deposition
(2004)We report the growth of single-phase, stoichiometric polycrystalline thin films of the half-Heusler ferromagnet NiMnSb, predicted to be half-metallic, on single crystal InSb (100) substrates heated at 200°C by pulsed laser ...
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Article
Studies of the tribological and mechanical properties of laminated CrC-SiC coatings produced by r.f. and d.c. sputtering
(1997)Multilayer CrC-SiC coatings were produced by both direct current and radio frequency sputtering of Cr and Si targets in an Ar-C2H2 atmosphere. Coatings of constant thickness of about 4 μm, but with the number of layers ...
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Article
Superhelices of poly[2-(acetoacetoxy)ethyl methacrylate]
(2004)Poly[2-(acetoacetoxy) ethyl methacrylate] (PAEMA) homopolymers were found to self-assemble into hierarchical superstructures, that is, double-stranded helical tubes of either screw sense (scanning force microscopy). Both ...
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Surface particularities in pulsed laser ablation/deposition of the ferromagnetic alloy NiMnSb
(2003)In this work we investigate the surface morphology and stoichiometry of the ablated targets employed with pulsed laser deposition (PLD) of thin films of the ferromagnetic half-Heusler alloy NiMnSb. The NiMnSb targets were: ...