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Browsing by Subject "synthesis"

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    • Article  

      A2Bi8Se13 (A = Rb, Cs), CsBi3.67Se6, and BaBi2Se4: New ternary semiconducting bismuth selenides 

      Iordanidis, L.; Brazis, P. W.; Kyratsi, Theodora; Ireland, J.; Lane, M.; Kannewurf, C. R.; Chen, W.; Dyck, J. S.; Uher, C.; Ghelani, N. A.; Hogan, T.; Kanatzidis, M. G. (2001)
      Rb2Bi8Se13 (I), Cs2Bi8Se13 (II), CsBi3.67Se6 (III), and BaBi2Se4 (IV) were synthesized by direct combination reactions of the A/Se (A = Rb, Cs, Ba) and Bi2Se3 at ≥650 °C. Their structures were determined by single-crystal ...

    • Article  

      Amphiphilic diblock and ABC triblock methacrylate copolymers: Synthesis and aqueous solution characterization 

      Triftaridou, Aggeliki I.; Vamvakaki, Maria; Patrickios, Costas S. (2002)
      Three isomeric, linear, equimolar, amphiphilic ABC triblock copolymers comprising methyl methacrylate (MMA, nonionic hydrophobic), 2-(dimethylamino)ethyl methacrylate, (DMAEMA, ionizable hydrophilic) and hexa(ethylene ...

    • Article  

      Broom-like and flower-like heterostructures of silver molybdate through pH controlled self assembly 

      Singh, D. P.; Sirota, B.; Talpatra, S.; Kohli, P.; Rebholz, Claus; Aouadi, S. M. (2012)
      Silver molybdate microrods are selfassembled into micron sized, broom-like and flowerlike structures. Our investigations indicate that through a simple hydrothermal process, large scale production of such structure is ...

    • Article  

      Cationic amphiphilic model networks based on symmetrical ABCBA pentablock terpolymers: Synthesis, characterization, and modelling 

      Triftaridou, Aggeliki I.; Vamvakaki, Maria; Patrickios, Costas S. (2007)
      Eight isomeric networks based on equimolar terpolymers were synthesized using group transfer polymerization (GTP) and were characterized in terms of their swelling properties. Two hydrophilic monomers, the nonionic methoxy ...

    • Article  

      Cationic double-hydrophilic model networks: Synthesis, characterization, modeling and protein adsorption studies 

      Loizou, Elena; Triftaridou, Aggeliki I.; Georgiou, Theoni K.; Vamvakaki, Maria; Patrickios, Costas S. (2003)
      Group transfer polymerization (GTP) was used for the preparation of eight networks based on two hydrophilic monomers, 2-(dimethylamino)ethyl methacrylate (DMAEMA) and poly(ethylene glycol) methacrylate (PEGMA). Ethylene ...

    • Article  

      Characterization and magnetic properties of a "super stable" radical 1,3-diphenyl-7-trifluoromethyl-1,4-dihydro-1,2,4-benzotriazin-4-yl 

      Constantinides, Christos P.; Koutentis, Panayiotis Andreas; Krassos, H.; Rawson, J. M.; Tasiopoulos, Anastasios J. (2011)
      1,3-Diphenyl-7-trifluoromethyl-1,4-dihydro-1,2,4-benzotriazin-4-yl (4), prepared in SSSShigh yield via the catalytic oxidation of the corresponding amidrazone 5 by using Pd/C (1.6 mol ss%) and 1,8-diazabicyclo[5.4.0]undec-7-ene ...

    • Article  

      Composite nanotubes formed by self-assembly of PbS nanoparticles 

      Leontidis, Epameinondas; Orphanou, M.; Kyprianidou-Leodidou, Tasoula; Krumeich, F.; Caseri, Walter (2003)
      Unusual arrangements of nanoparticles were observed during the synthesis and subsequent dissolution of PbS particles under the action of the surfactant sodium dodecyl sulfate (SDS) in solutions containing hydrophilic ...

    • Article  

      Concerted Diels-Alder reaction between anthracene and C60 

      Chronakis, Nikos; Orfanopoulos, Michael (2001)
      The Diels-Alder reaction of anthracene with C60 has been investigated experimentally by using secondary isotope effects. The inverse α-secondary isotope effect in conjunction with the unity value of the β-secondary isotope ...

    • Article  

      Controlled synthesis of homopolymers and block copolymers based on 2-(acetoacetoxy)ethyl methacrylate via RAFT radical polymerisation 

      Krasia-Christoforou, T.; Soula, R.; Börner, H. G.; Schlaad, H. (2003)
      Reversible addition-fragmentation chain transfer (RAFT) radical polymerisation enables to synthesise well-defined homopolymers and block copolymers based on 2-(acetoacetoxy)ethyl methacrylate, which are capable to strongly ...

    • Article  

      Correlations of synthetic, spectroscopic, structural, and speciation studies in the biologically relevant Cobalt(II) - Citrate system: The tale of the first aqueous dinuclear Cobalt(II) - Citrate complex 

      Kotsakis, N.; Raptopoulou, C. P.; Tangoulis, V.; Terzis, A.; Giapintzakis, John; Jakusch, T.; Kiss, T.; Salifoglou, A. (2003)
      Synthetic efforts targeting soluble species of Co(II) with the low molecular mass physiological ligand citric acid led to the isolation of the first dinuclear complex [Co2(C6H5O7)2 (H2O)4]2-, at pH ∼5, in the form of its ...

    • Article  

      CsMBi3Te6 and CsM2Bi3Te7 (M = Pb, Sn): New thermoelectric compounds with low-dimensional structures 

      Hsu, K. F.; Chung, D. Y.; Lal, S.; Mrotzek, A.; Kyratsi, Theodora; Hogan, T.; Kanatzidis, M. G. (2002)
      The new materials CsPbBi3Te6 nad CsPb2Bi3Te7 were discovered through reactions of CsBi4Te6 with PbTe, whereas the isostructural materials CsSnBi3Te6 and CsSn2Bi3Te7 were discovered through corresponding reactions with SnTe. ...

    • Article  

      Design and synthesis of new nanosized C 3-symmetrical tricarboxylic acids: Key elongated ligands for the preparation of highly porous MOFs 

      Markoulides, Marios Savva; Efthymiou, Constantinos G.; Tasiopoulos, Anastasios J.; Chronakis, Nikos (2015)
      The synthesis of two new C 3-symmetrical nanosized tricarboxylic acids bearing triphenylmethane cores and three imines linkages is presented. The new elongated tripods were designed to stabilise highly porous metal-organic ...

    • Article  

      Detosylation of 3-amino-1-tosylindole-2-carbonitriles using DBU and thiophenol 

      Michaelidou, Sophia S.; Koutentis, Panayiotis Andreas (2010)
      Attempted detosylation of the 3-amino-1-(p-tosylamino)indole-2-carbonitriles 4a-c using either K2CO3 in EtOH or DBU in PhH at reflux gives unexpectedly the 3-(N-p-tosylamino)indole-2-carbonitriles 5a-c, respectively in ...

    • Article  

      A dimethacrylate cross-linker cleavable under thermolysis or alkaline hydrolysis conditions: Synthesis, polymerization, and degradation 

      Elladiou, Marios; Patrickios, Costas S. (2016)
      We develop a new platform based on 2,6-pyridinediethanol diesters for introducing polymer degradability under thermolysis or alkaline hydrolysis conditions, with the latter being rare in polymers. Such labile diesters can ...

    • Article  

      Effects of sol-gel synthesis on 5Fe-15Mn-40Zn-40Ti-O mixed oxide structure and its H2S removal efficiency from industrial gas streams 

      Polychronopoulou, Kyriaki; Efstathiou, Angelos M. (2009)
      A novel Fe-Mn-Zn-Ti-O mixed metal oxide has been developed for efficient low-temperature (25-50°C) removal of H2S from a gas mixture containing 600 ppm H2S, 25 vol% H2, 7.5 vol % CO 2, and 1-3 vol% H2O that simulates typical ...

    • Article  

      Employment of methyl 2-pyridyl ketone oxime in manganese non-carboxylate chemistry: MnII2MnIV and MnII 2MnIII6 complexes 

      Stoumpos, Constantinos C.; Stamatatos, Theocharis C.; Sartzi, H.; Roubeau, O.; Tasiopoulos, Anastasios J.; Nastopoulos, Vassilios; Teat, S. J.; Christou, George; Perlepes, Spyros P. (2009)
      The employment of the anion of methyl 2-pyridyl ketone oxime (mpko -) as a tridentate chelating/bridging ligand in manganese chemistry is described. The inorganic anion (Br-, ClO4-) used in the reaction affects the identity ...

    • Article  

      Enantioseparations in open-tubular capillary electrochromatography: Recent advances and applications 

      Kapnissi‐Christodoulou, Constantina P.; Nicolaou, Athina G.; Stavrou, Ioannis J. (2016)
      This review highlights recent advances and applications in open-tubular capillary electrochromatography (OT-CEC) for enantioseparations during the last decade. Although extensive research has been conducted in the area of ...

    • Article  

      The first one-pot synthesis of a chiral pentakis-adduct of C60 utilising an opened-structure malonate tether 

      Ioannou, Charalambos P.; Chronakis, Nikos (2013)
      A pentakis-adduct of C60 with an incomplete octahedral addition pattern was synthesised via a one-pot procedure using a tether equipped with five malonate moieties. The five-fold Bingel cyclopropanation of C60 was completely ...

    • Article  

      Formation of oligotriazoles catalysed by cucurbituril 

      Krasia-Christoforou, T.; Steinke, J. H. G. (2002)
      The catalytic activity of cucurbituril in 1,3-dipolar cycloadditions has been applied to the synthesis of oligotriazoles.

    • Article  

      Halogen derivatives of m-phenylene(carbeno)nitrene: A switch in ground-state multiplicity 

      Enyo, T.; Nicolaïdes, Andrew N.; Tomioka, H. (2002)
      m-Phenylene-coupled carbenonitrenes [(3-nitrenophenyl)methylene (2-H), (3-nitrenophenyl)fluoromethylene (2-F), (3-nitrenophenyl)chloromethylene (2-Cl), (3-nitrenophenyl)bromomethylene (2-Br)] have been investigated ...

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